Electrical Mode (DC)

Soft ResiScope™

True Quantitative Resistance/Current Measurements with Intermittent Contact

Soft ResiScope™ is an AFM mode for quantitative resistance and current measurements on soft and fragile conductive samples. It combines intermittent contact with ResiScope™ measurements, for the electrical characterization of sensitive materials.

In short

  • Soft ResiScope™ measures resistance and current from 10² to 10¹² Ω on soft and fragile conductive samples, using intermittent contact instead of continuous contact.
  • The tip touches each point with a constant force and is never dragged across the surface: no friction, no sample damage from shear and less tip wear.

CSInstruments · Updated

Soft Interaction Control

The switch happens mid-scan

On a battery electrode, the scan changes from contact ResiScope to Soft Interaction Control halfway through: Soft IC improves the measurement without scratching the surface.

  • No shear on the particle, no scratching
  • Structure inside the particle becomes readable
  • Resistance: 314 kΩ to 902 GΩ

Application fields

Soft ResiScope™ is for samples that contact mode would scratch or push aside: battery electrodes and separators, solid electrolytes, organic films, polymers, 2D materials and biological samples.

Key Features

Soft ResiScope

  • Non-Destructive Measurements: Ideal for fragile and soft conductive samples
  • Wide Measurement Range: Resistance from 10² to 10¹² ohms
  • No Friction: Prevents sample damage and tip wear
  • Constant Force: Ensures quantitative electrical measurements
  • Intermittent Contact: Optimizes electrical measurement while preserving tip and sample integrity
Soft ResiScope™ on VO₂: topography and resistance, 10 µm

Soft Intermittent Contact : The 3rd AFM mode

  • Combines precision of contact AFM with dynamic capabilities of resonant modes
  • Ideal for delicate and soft materials
  • Detailed mechanical and electrical measurements with minimal sample disturbance
  • \1, Soft PFM, Soft ResiScope and Soft SThM
Adhesion Stiffness analysis with AFM

Soft IC Mode

  • Adhesion
  • Stiffness
  • Young’s Modulus

Soft ResiScope

  • Integrates intermittent contact AFM with detailed resistance and current mapping
  • Wide range of resistance measurements (10² to 10¹² ohms)
  • Excellent for fragile conductive samples and advanced material studies
Mechanical analysis of sample with AFM

Gallery

ResiScope™ results

How does Soft ResiScope work?

Soft ResiScope operates on an intermittent contact principle:

  1. The AFM probe makes brief, controlled contact with the sample
  2. During contact, a constant force is applied, allowing precise resistance and current measurements
  3. The tip is then retracted and moved to the next measurement point
  4. This cycle repeats, creating a comprehensive map of electrical properties without damaging the sample
Soft ResiScope operates on an intermittent contact principle: – Soft ResiScope™

Specifications

  • Measurement Range: 10² to 10¹² ohms
  • Compatibility: Nano-Observer AFM systems
  • Supported Modes: Intermittent contact
  • Data Output: Simultaneous topography and electrical property mapping

Quantitative Measurements

Resistance signal, 5μm scan, Soft ResiScope mode
Ultrathin granular gold layer evaporated on a doped-Si substrate: Resistance signal, 5μm scan

Soft ResiScope provides quantitative measurements comparable to standard ResiScope in contact mode:

  • Identical Results: Topography and resistance signals match between Soft ResiScope and contact mode ResiScope on standard electrical samples (e.g., SRAM)
  • High Resolution: Maintains lateral resolution while ensuring quantitative measurements

Advantages Over Traditional Methods

Compared with contact-mode ResiScope™, Soft ResiScope™ removes friction, which protects both the sample and the tip. On fragile samples it gives images comparable to oscillating mode, with a resistance value at every point.

Soft ResiScope vs. Standard ResiScope

Soft ResiScope vs ResiScope
Section comparison

Soft ResiScope vs. Oscillating/Contact Modes

  • Sample Preservation: Prevents surface damage common in contact mode
  • Equivalent Results: Produces data comparable to oscillating mode on fragile samples
  • Versatility: Suitable for a wide range of materials, from polymers to biological samples

Questions about Soft ResiScope™?

Ask the application scientists behind our AFMs and modes, about your samples, probes, set-up or which mode fits your measurement. We answer every message personally.